Grain Size Control of the Magnetic Nanoparticles by Solid State Route Modification

Abstract

The CoFe2O4 and NiFe2O4 nanoparticles were synthesized exploiting a co-precipitation method and afterward calcinated at 400 A degrees C through two different experimental apparatus: a conventional muffle and rotatory oven. X-ray diffraction (XRD) analysis revealed that nanocrystalline ferrites grew with a face center cubic structure (fcc) and Fd3m symmetry space group. XRD, transmission electron microscopy, and magnetic measurements confirmed the compositional homogeneity and the narrow size particle distribution (6-8 nm) of the sample thermally treated in a rotary oven, in all likelihood due to the sample's constant turning movement. The size of the magnetic particles is extremely important and influences the choice of a potential technological application. For this reason, our study emerges as a new and simple innovating procedure to control the size of magnetic nanoparticles.


Autore Pugliese

Tutti gli autori

  • Barreto A. C. H.; Santiago V. R.; Freire R. M.; Mazzetto S. E.; Sasaki J. M.; Vasconcelos I. F.; Denardin J. C.; Mele G.; Carbone L.; Fechine P. B. A.

Titolo volume/Rivista

Journal of materials engineering and performance


Anno di pubblicazione

2013

ISSN

1059-9495

ISBN

Non Disponibile


Numero di citazioni Wos

Nessuna citazione

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Numero di citazioni Scopus

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Settori ERC

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Codici ASJC

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