Rapid prediction of deoxynivalenol contamination in wheat bran by MOS-based electronic nose and characterization of the relevant pattern of volatile compounds

Abstract

Deoxynivalenol (DON) is a mycotoxin, mainly produced by Fusarium sp., most frequently occurring in cereals and cereal-based products. Wheat bran refers to the outer layers of the kernel, which has a high risk of damage due to chemical hazards, including mycotoxins. Rapid methods for DON detection in wheat bran are required.RESULTSA rapid screening method using an electronic nose (e-nose), based on metal oxide semiconductor sensors, has been developed to distinguish wheat bran samples with different levels of DON contamination. A total of 470 naturally contaminated wheat bran samples were analyzed by e-nose analysis. Wheat bran samples were divided in two contamination classes: class A ([DON] 400 mu g kg(-1), 225 samples) and class B ([DON] > 400 mu g kg(-1), 245 samples). Discriminant function analysis (DFA) classified wheat bran samples with good mean recognizability in terms of both calibration (92%) and validation (89%). A pattern of 17 volatile compounds of wheat bran samples that were associated (positively or negatively) with DON content was also characterized by HS-SPME/GC-MS.


Tutti gli autori

  • Lippolis V.; Cervellieri S.; Damascelli A.; Pascale M.; Di Gioia A.; Longobardi F.; De Girolamo A.

Titolo volume/Rivista

Journal of the Science of Food and Agriculture


Anno di pubblicazione

2018

ISSN

0022-5142

ISBN

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