MZnFe2O4 (M = Ni, Mn) cubic superparamagnetic nanoparticles obtained by hydrothermal synthesis
Abstract
MZnFe2O4 (M = Ni or Mn) cubic nanoparticles have been prepared by hydrothermal synthesis in mild conditions and short time without any procedure of calcinations. The structural and magnetic properties of the mixed ferrites were investigated by X-ray diffraction, Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy, Mössbauer spectroscopy, vibrating sample magnetometer, and Transmission electron microscopy (TEM). X-ray analysis showed peaks characteristics of the spinel phase. The average diameter of the nanoparticles observed by TEM measurements was approximately between 4 and 10 nm. Spectroscopy study of the spinel structure was performed based on Group Theory. The predicted bands were observed in FTIR and Raman spectrum. The magnetic parameters and Mössbauer spectroscopy were measured at room temperature and superparamagnetic behavior was observed for mixed ferrites. This kind of nanoparticles can be used as precursor in drug delivery systems, magnetic hyperthermia, ferrofluids, or magnetic imaging contrast agents.
Autore Pugliese
Tutti gli autori
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R. M. Freire , T. S. Ribeiro , I. F. Vasconcelos , J. C. Denardin , E. B. Barros , Giuseppe Mele , L. Carbone , S. E. Mazzetto , P. B. A. Fechine
Titolo volume/Rivista
JOURNAL OF NANOPARTICLE RESEARCH
Anno di pubblicazione
2013
ISSN
1388-0764
ISBN
Non Disponibile
Numero di citazioni Wos
Nessuna citazione
Ultimo Aggiornamento Citazioni
Non Disponibile
Numero di citazioni Scopus
19
Ultimo Aggiornamento Citazioni
24/04/2018
Settori ERC
Non Disponibile
Codici ASJC
Non Disponibile
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