Influence of glass phase on Al2O3 fiber-reinforced Al2O3 composites processed by slip casting

Abstract

The present work describes the processing of alumina fiber reinforced alumina ceramic preforms consisting of chopped Al2O3 fibers (33 wt%) and Al2O3 (67 wt%) fine powders by slip casting. The preforms were pre-sintered in air at 1100 °C for 1 h. A lanthanum based glass was infiltrated into these preforms at 1250 °C for 90 min. Linear shrinkage (%) was studied before and after glass infiltration. Pre-sintered and infiltrated specimens were characterized by scanning electron microscopy, energy dispersive X-ray, X-ray diffraction, porosimetry and flexural strength. The alumina preforms showed a narrow pore size distribution with an average pore size of ∼50 nm. It was observed that introducing Al2O3 fibers into Al2O3 particulate matrix produced warp free preforms with minor shrinkage during pre-sintering and glass infiltration. It was observed that the infiltration process fills up the pores and considerably improves the strength and reliability of alumina preform.


Tutti gli autori

  • A. Licciulli , V. Contaldi , S. Kunjalukkal Padmanabhan , A. Balakrishnan , C. Siligardi , D. Diso

Titolo volume/Rivista

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY


Anno di pubblicazione

2011

ISSN

0955-2219

ISBN

Non Disponibile


Numero di citazioni Wos

Nessuna citazione

Ultimo Aggiornamento Citazioni

Non Disponibile


Numero di citazioni Scopus

6

Ultimo Aggiornamento Citazioni

28/04/2018


Settori ERC

Non Disponibile

Codici ASJC

Non Disponibile