A combined PIXE–PIGE approach for the assessment of the diagenetic state of cremated bones submitted to AMS radiocarbon dating

Abstract

Bone samples from a Bronze age necropolis in Northern Italy, exposed to different combustion temperatures,were submitted to XRD (X-ray Diffraction), PIXE (Particle Induced X-ray Emission) and PIGE (Particle Induced Gamma Ray Emission) analyses in order to obtain information about their diagenetic state. Structural carbonate was then extracted by acid hydrolysis and used for 14C-AMS (Accelerator Mass Spectrometry) dating. These analytical techniques permitted the study of the effects of the combustion temperature on the crystallinity of the bone apatite and on its elemental chemical composition in terms of major, minor and trace elements. The results indicate that combustion at temperatures above 700 C induces changes in the bone crystalline structure, reducing the diagenetic uptake of elements from the burial environment.


Tutti gli autori

  • G. Quarta , L. Calcagnile , M. D'Elia , L. Maruccio , V. Gaballo , A. Caramia

Titolo volume/Rivista

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH. SECTION B, BEAM INTERACTIONS WITH MATERIALS AND ATOMS


Anno di pubblicazione

2013

ISSN

0168-583X

ISBN

Non Disponibile


Numero di citazioni Wos

4

Ultimo Aggiornamento Citazioni

28/04/2018


Numero di citazioni Scopus

4

Ultimo Aggiornamento Citazioni

28/04/2018


Settori ERC

Non Disponibile

Codici ASJC

Non Disponibile